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The HPLC column Kinetex ® 2.6 μm XB-C18 100 Å (30 ∗ 2.1 mm) was purchased from Phenomenex (Torrance, CA, United States), and the HPLC column Mediterranea Sea 18 column (10 ∗ 0.2 cm, 2.2 μm) was purchased from Teknokroma (Sant Cugat del Vallès, Spain). HPLC-MS Analysis
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